gamma-sitosterol and acteoside

From the methanolic extract of the roots of Clerodendrum philipinum, a new rearranged abietane diterpene (1) and eight known compounds were isolated by various chromatography methods. Their structures were identified by means of spectroscopic methods, including 1D- and 2D-NMR, as 17(15-->16),18(4-->3)-bisabeo-11,12,14,16-tetrahydroxy-3,5,8,11,13,15-abietahexaen-7-one (1), binankadsurin A, clerodenoside A, martynoside, acteoside, isoacteoside, astragalin, p3-sitosterol, and daucosterol. Binankadsurin A was found for the first time from a Clerodendrum species.

Topics: Abietanes; Chromatography; Clerodendrum; Glucosides; Kaempferols; Lignans; Magnetic Resonance Spectroscopy; Methanol; Molecular Structure; Phenols; Sitosterols

To study the chemical constituents from Lamium maculatum L. var Kansuense.. The chemical constituents were isolated and repeatedly purified by silica gel column chromatography and the structures were elucidated by the NMR spectra and physico-chemical properties.. Ten compounds were obtained and they were identified as D-mannitol, beta-sitosterol, stigmasterol, rutin, 3'-methylquercetin-3-O-rutinoside, n-butyl-beta-D-fructopyranoside, daucosterol, acteoside, 20-hydroxyecdysone, allantoin.. All the compounds were obtained from L. maculatum L. var Kansuense for the first time.

Topics: Allantoin; Ecdysterone; Glucosides; Lamiaceae; Mannitol; Phenols; Plants, Medicinal; Rutin; Sitosterols; Stigmasterol

To separate and identify the constituents from Clerodendron fragrans.. The constituents were isolated and purified with chromatographic methods, identified by NMR, MS, IR.. Beta-sitosterol (1), clerosterol (2), daucosterol (3), caffeic acid (4), kaempferol (5), 5,4'-dihydroxy-kaempferol-7-O-beta-rutinoside (6), acteoside (7) and leucoseceptoside A (8), were isolated and identified.. Compound 7 and 8 were identified for the first time from Clerodendron fragrans.

Topics: Clerodendrum; Glucosides; Glycosides; Phenols; Plant Leaves; Plants, Medicinal; Sitosterols

To study the chemical constituents in the leaf of Ligustrum delavayanum Hariot.. The constituents were isolated with column chromatographies and the structures were identified by MS, IR, UV and NMR.. Four compounds were isolated and identified as beta-sitosterol, oleanic acid, 2 alpha-hydroxyursolic acid, and acteoside.. All the compounds were isolated from the plant for the first time.

Topics: Glucosides; Ligustrum; Oleanolic Acid; Phenols; Plant Leaves; Plants, Medicinal; Sitosterols