calpain and isobutyl-chloroformate

calpain has been researched along with isobutyl-chloroformate* in 1 studies

Other Studies

1 other study(ies) available for calpain and isobutyl-chloroformate

Article	Year
Unprecedented crystallization and X-ray crystal structure of racemic N(alpha)-(t-butyloxycarbonyl)-L-L-phenylalanine N-methoxy-N-methylamide. Chirality, 2000, Volume: 12, Issue:1 Weinreb amide 3 was synthesized using isobutyl chloroformate, carbonyldiimidazole, or ethylcarbodiimide as the coupling agent in the reaction of Boc-phenylalanine with O,N-dimethylhydroxylamine hydrochloride. An optically active oil was isolated along with an optically inactive solid irrespective of the type of coupling agent used. Single crystal X-ray analysis of the solid revealed that it is a racemate. The molecular packing of the crystals reflect the stability of the racemate as opposed to an enantiomerically pure solid. Topics: Calpain; Carbodiimides; Cross-Linking Reagents; Crystallography, X-Ray; Cysteine Proteinase Inhibitors; Formates; Molecular Weight; Phenylalanine; Stereoisomerism	2000

Article

Year

Unprecedented crystallization and X-ray crystal structure of racemic N(alpha)-(t-butyloxycarbonyl)-L-L-phenylalanine N-methoxy-N-methylamide.

Chirality, 2000, Volume: 12, Issue:1

Weinreb amide 3 was synthesized using isobutyl chloroformate, carbonyldiimidazole, or ethylcarbodiimide as the coupling agent in the reaction of Boc-phenylalanine with O,N-dimethylhydroxylamine hydrochloride. An optically active oil was isolated along with an optically inactive solid irrespective of the type of coupling agent used. Single crystal X-ray analysis of the solid revealed that it is a racemate. The molecular packing of the crystals reflect the stability of the racemate as opposed to an enantiomerically pure solid.

Topics: Calpain; Carbodiimides; Cross-Linking Reagents; Crystallography, X-Ray; Cysteine Proteinase Inhibitors; Formates; Molecular Weight; Phenylalanine; Stereoisomerism

2000